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sec-butyl disulfide CAS 5943-30-6

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Chemical Name: sec-butyl disulfide

Synonyms: Di-Sec-butyldisulfide , bis(sec-butyl) disulphide

CAS No.: 5943-30-6

Molecular Formula: C8H18S2

Molecular Weight: 176.36g/mol

Appearance: Colorless liquid

Purity: 98.5%min

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sec-butyl disulfide quick Details

Chemical Name: sec-butyl disulfide

Synonyms: Di-Sec-butyldisulfide , bis(sec-butyl) disulphide

CAS-No.: 5943-30-6

Molecular Formula: C8H18S2

Molecular Weight: 176.36g/mol

Molecular structure: image.png

Density: 0.957 g/cm3

Melting point: -49°C

Boiling point: 220.6°C

Flash point: 67.2 °C –closed cup

Solubility: Soluble in ethanol and ether, insoluble in water.

sec-butyl disulfide typical Properties

ItemIndex
AppearanceColorless liquid
Purity98.5%min
Water0.1%max

sec-butyl disulfide Usage

This product is mainly used as organic intermediate.

sec-butyl disulfide Packaging

180Kg/drum, or according to the customer request.

sec-butyl disulfide Storage

Keep airtight in a dry and cool place.

sec-butyl disulfide Preparation or source

(1) The corresponding bromobutane and sodium sulfide were refluxed into ethanol.

(2) The corresponding butanol and carbon disulfide were heated and refluxed. 

(3) Using corresponding butanol and hydrogen sulfide as raw materials, heated under the catalysis of gamma-alumina, prepared by gas-solid catalytic reaction.

A Small Method for Preparing Disec-Butyl Disulfide

1. Sodium sulfide and water were added into the reaction bottle, after stirring and dissolving, sulfur powder was added, heated to 55 C under stirring for 1 hour, then cooled. 

2. The obtained water solution was transferred to the microwave reactor, quaternary ammonium salt phase transfer catalyst was added, and 2-Bromobutane was added. 

3. The microwave reactor was opened and stirred for 0.2-2 hours at 300-1000W power to terminate the reaction. Disec-butyl disulfide was synthesized from the reaction liquid by standing, separating the water phase and distilling the organic phase.

Remarks

Isomers of dibutyl sulfide. It's stimulating.

sec-butyl disulfide Packaging and Shipping

Packing: 25Kg/drum

Delivery: delivery within 3-5working days.

sec-butyl disulfide Storage

Avoiding light and drying.

First-aid measures

4.1Description of necessary first-aid measures

General advice

Consult a physician. Show this safety data sheet to the doctor in attendance.

If inhaled

If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician.

In case of skin contact

Wash off with soap and plenty of water. Consult a physician.

In case of eye contact

Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician.

If swallowed

Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.

4.2Most important symptoms/effects, acute and delayed

no data available

4.3Indication of immediate medical attention and special treatment needed, if necessary

no data available

 

Fire-fighting measures

5.1Extinguishing media

Suitable extinguishing media

Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.

5.2Specific hazards arising from the chemical

no data available

5.3Special protective actions for fire-fighters

Wear self-contained breathing apparatus for firefighting if necessary.

6.Accidental release measures

6.1Personal precautions, protective equipment and emergency procedures

Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8.

6.2Environmental precautions

Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment must be avoided.

6.3Methods and materials for containment and cleaning up

Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

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